P,P′-(9,9-二甲基-9H-氧雜蒽-4,5-二基)雙[N,N,N′,N′-四乙基-亞膦酸二酰胺]的合成路線

提問時間：2021/4/26 8:22:06

P,P′-(9,9-二甲基-9H-氧雜蒽-4,5-二基)雙[N,N,N′,N′-四乙基-亞膦酸二酰胺]是什么，有什么方法可以合成？

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匿名

2021/4/26 8:22:06

基本信息：
中文名稱 P,P′-(9,9-二甲基-9H-氧雜蒽-4,5-二基)雙[N,N,N′,N′-四乙基-亞膦酸二酰胺]
中文別名 XANTPHOS BASED LIGAND;
英文名稱 N-[[5-[bis(diethylamino)phosphanyl]-9,9-dimethylxanthen-4-yl]-(diethylamino)phosphanyl]-N-ethylethanamine
英文別名 9,9-DIMETHYL-4,5-BIS(BIS(DIETHYLAMIDO)PHOSPHINO)XANTHENE;P,P''-(9,9-DIMETHYL-9H-XANTHENE-4,5-DIYL)BIS[N,N,N'',N''-TETRAETHYL-PHOSPHONOUS DIAMIDE];Xantphos based ligand;4,5-(bis[bis-diethylamido]phosphonito)-9,9-dimethylxanthene;P,P inverted exclamation marka-(9,9-Dimethyl-9H-xanthene-4,5-diyl)bis[N,N,N inverted exclamation marka,N inverted exclamation marka-tetraethyl-phosphonous diamide];4,5-bis[bis(diethylamino)phosphino]-9,9-dimethylxanthene;4,5-(Bis[bis-diethylamino]phosphonito)-9,9-dimethylxanthene;4,5-(bis[bis-diethylamido]phosphonito)-9,9-dimethyl-9H-xanthene;
CAS號 349100-75-0

合成路線：
1.通過9,9-二甲基氧雜蒽和雙(二乙基氨基)氯膦合成P,P′-(9,9-二甲基-9H-氧雜蒽-4,5-二基)雙[N,N,N′,N′-四乙基-亞膦酸二酰胺]，收率約64%；